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ChemInform Abstract: A Versatile and Practical Synthesis of α-Trifluoromethylated Alcohols from Trifluoroacetaldehyde Ethyl Hemiacetal in Water.

✍ Scribed by T.-P. LOH; X.-R. LI

Book ID
112040685
Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
27
Category
Article
ISSN
0931-7597

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📜 SIMILAR VOLUMES

A simple and practical synthesis of α-tr
A simple and practical synthesis of α-trifluoromethylated alcohols in water
✍ Teck-Peng Loh; Xu-Ran Li 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 635 KB

A simple and practical preparation of a-trifluoromethylated alcohols in water v/a indium-mediated allylation reaction and tin-mediated indium trichloride-promoted ailylation reaction of trifluoroacetaldehyde hydrate and its ethyl hcmiacetal is described in this paper.

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ChemInform Abstract: A Versatile Approach to 2-Substituted 3-Trifluoromethyl-1,3-diols Based on the Reaction of Trifluoroacetaldehyde Ethyl Hemiacetal with Enamines Derived from Aldehydes.
✍ Kazumasa Funabiki; Yudai Furuno; Fumiaki Sato; Hiroshi Gonda; Yasuhiro Kubota; M 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 79 KB

## Abstract The reaction of enamine (I) with ethyl hemiacetal (II) followed by acid hydrolysis and subsequent reduction of the intermediate aldehyde gives rise to the diastereomeric mixture of diols (III) and (IV).