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ChemInform Abstract: A New Synthetic Route to β-2′-Deoxyribosyl-5-substituted Pyrrolo( 2,3-d)pyrimidines. Synthesis of 2′-Deoxycadeguomycin.

✍ Scribed by E. D. EDSTROM; Y. WEI

Book ID
112023888
Publisher
John Wiley and Sons
Year
2010
Weight
41 KB
Volume
26
Category
Article
ISSN
0931-7597

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A new and versatile synthesis of 5-subst
A new and versatile synthesis of 5-substituted pyrrolo[2,3-d]pyrimidines
✍ Dolorès Edmont; David M Williams 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 80 KB

We have developed a new methodology for the construction of 5-substituted pyrrolo [2,3-d]pyrimidines that involves the reduction of a nitroalkane to an oxime using the reducing ability of the Sn(SR 3 ) -species, followed by mild, acid-catalysed deoximation of the resulting adduct using Dowex-H + res