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ChemInform Abstract: A Modified Sandmeyer Methodology and the Synthesis of (.+-.)- Convolutamydine A.

✍ Scribed by S. J. GARDEN; J. C. TORRES; A. A. FERREIRA; R. B. SILVA; A. C. PINTO

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

A Modified Sandmeyer Methodology and the Synthesis of (Β±)-Convolutamydine A.

-A modified Sandmeyer methodology (lower temperature and addition of ethanol) is found to be useful for the high yield synthesis of Ξ±-isonitrosoacetanilides (III). Derivative (IIIc) is readily converted to (Β±)-convolutamydine A (VI). The analogous 5,7-dibromo derivative (IX) is obtained from isatin (VII). -(GARDEN, S.

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