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Chemical Synthesis and Quantitative Estimation of 3-Deoxy d-manno-Octulosonic Acid

✍ Scribed by D. Charon; R. S. Sarfati; D. R. Strobach; L. Szabó

Book ID
115112072
Publisher
John Wiley and Sons
Year
1969
Tongue
English
Weight
634 KB
Volume
11
Category
Article
ISSN
1432-1327

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KDO (1) is synthesized in five steps, starting from 1,2-to the carbonate 9. Silicon-induced lactonization affords the lactone 10, which can be converted into NH 4 -KDO by anhydro-3,4:5,6-di-O-isopropylidene-D-mannitol ( 6). The epoxide 6, obtained from D-mannitol (2), reacts with lithiated standard