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catena-Poly[silver(I)-μ-4-aminobenzenesulfonato-μ-2,3-diethylpyrazine]

✍ Scribed by Liu, Hai-Yan ;Ma, Ji-Cheng ;Yang, Jin

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
349 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, [Ag(C~6~H~6~NO~3~S)(C~8~H~8~N~2~)], the Ag^I^ cation is four-coordinated by three N atoms from two different 2,3-diethylpyrazine ligands and one –NH~2~ group of a 4-aminobenzenesulfonate ligand, and one sulfonate O atom in a distorted tetrahedral coordination geometry. The Ag^I^ centers are doubly bridged by both types of ligands, forming a one-dimensional chain. N—H...O hydrogen bonds complete the structure.

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The title complex, [AgKCl 2 (C 12 H 24 O 6 )] n , has been synthesized by reaction of 18-crown-6 with KCl and AgNO 3 . [K(18crown-6)] + cations and [AgCl 2 ] À anions form one-dimensional chains through KÁ Á ÁCl interactions of length 3.2568 (14) A ˚. Both the K + and the Ag I ions lie on centres of