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Cascade Cyclizations of Acyclic and Macrocyclic Alkynones: Studies toward the Synthesis of Phomactin A

โœ Scribed by Ciesielski, Jennifer; Gandon, Vincent; Frontier, Alison J.

Book ID
120426096
Publisher
American Chemical Society
Year
2013
Tongue
English
Weight
588 KB
Volume
78
Category
Article
ISSN
0022-3263

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โœ Ian Paterson; Rebecca E Brown; Christopher J Urch ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 255 KB

The 14-membered macrocycle 3, an advanced intermediate in a synthetic approach to lophotoxin, was prepared from stannane 20 using an intramolecular Stille coupling. The acyclic structural analogues 6 and 7 were obtained by analogous intermolecular coupling reactions.