Carbonylation of 2-chloro-4,6-dimethoxypyrimidine and 2-(chloromethy)-4,6-dimethoxypyrimidine
β Scribed by Yves Bessard; Roger Crettaz
- Book ID
- 108379162
- Publisher
- Elsevier Science
- Year
- 1999
- Tongue
- French
- Weight
- 388 KB
- Volume
- 55
- Category
- Article
- ISSN
- 0040-4020
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Contains A Database Of Approximately 70,000 Reactions And 4000 Of The Most Frequently Consulted Reagents. Fully Searchable By Structure And Sub-structure, Reagent, Reaction Type, Experimental Conditions, And Keyword. Also Includes A Searchable Interface: Acronym Finder (an Interface For Scientific A
The title compound, C 19 H 16 N 4 O 5 S, was synthesized by the reaction of 2-(4,6-dimethoxypyrimidine-2-ylsulfanyl)benzoic acid and 3-nitroaniline in the presence of N,N 0 -dicyclohexylcarbodiimide catalyst in dichloromethane. Intramolecular N-HΓ Γ ΓN hydrogen bonds are found in the crystal structu
## Abstract A convenient preparation of 2β[^15^N]βaminoβ4,6βdimethoxypyrimidine using ^15^Nβammonium chloride as the source of ^15^N is described.