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Carbon-13 labeled benzo[a]pyrenes and derivatives. 4. Labeling the 7-10 positions

✍ Scribed by Klassen, Sandra E.; Daub, Guido H.; VanderJagt, David L.


Book ID
126937340
Publisher
American Chemical Society
Year
1983
Tongue
English
Weight
942 KB
Volume
48
Category
Article
ISSN
0022-3263

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13C labeled benzo[a]pyrenes and derivati
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## Abstract The synthesis of benzo[a]pyrene‐6‐^13^C is described. Perinaphthane was converted to 6‐benzoyl‐carbonyl‐^13^C‐perinaphthane which was cyclized to 2,3‐dihydrobenzo[a]pyren‐6(1H)‐one‐6‐^13^C. Subsequent reduction of the ketone followed by dehydration and dehydrogenation gave benzo[a]pyren

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