✦ LIBER ✦

Capillary gas chromatography and mass spectrometry detection of anabolic steroids II

✍ Scribed by Cartoni, G. P. ;Giarrusso, A. ;Ciardi, M. ;Rosati, F.

Publisher: John Wiley and Sons
Year: 1985
Tongue: English
Weight: 401 KB
Volume: 8
Category: Article
ISSN: 0935-6304
DOI: 10.1002/jhrc.1240080912

No coin nor oath required. For personal study only.

✦ Synopsis

High resolution gas chromatography-mass spectrometry has been used to detect anabolic steroids in urine. With fused silica capillary columns connected directly to mass spectrometer, the anabolic steroids could be detected after extraction, hydrolysis, and derivatization with a sensitivity betterthen 1 ppb. fn vivo excretion and metabolism has been investigated for androstanolone, methandriol, oxymesterone, quindenione, and boldenone. permits solvent gradient elution at flow rates less than 10 pl/min with satisfactory reproducibility. chromatography (HPLC) and has been examined also in micro HPLC [1,2]. Micro columns facilitate temperature

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