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Capillary gas chromatographic determination of proteins and biological amino acids as N(O)-tert.-butyldimethylsilyl derivatives

✍ Scribed by Kang Lyung Woo; Dong Sun Lee

Publisher: Elsevier Science
Year: 1995
Weight: 592 KB
Volume: 665
Category: Article
ISSN: 0378-4347
DOI: 10.1016/0378-4347(94)00515-7

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## Abstract A simple, single‐step derivatization technique is presented for capillary GC‐FID and GC‐MS separation and identification of common protein and non‐protein constituents of natural peptides as their __tert__‐butyldimethylsilyl (TBDMS) derivatives. The __tert__‐butyldimethyl‐silylation of