𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Capillary gas chromatography of protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives in aqueous samples

✍ Scribed by Kyoung-Rae Kim; Jung-Han Kim; Chang-Hwan Oh; Tom J. Mabry

Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
694 KB
Volume
605
Category
Article
ISSN
1873-3778

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Analysis of all protein amino acids as t
Analysis of all protein amino acids as their tert.-butyldimethylsilyl derivatives by gas-liquid chromatography
✍ Chin-Joo Goh; Kenneth G. Craven; James R. Lepock; Erwin B. Dumbroff 📂 Article 📅 1987 🏛 Elsevier Science 🌐 English ⚖ 491 KB

A gas chromatographic method for the separation and quantitation of the 20 protein amino acids is described using N-methyl-N(tert.-butyldimethylsilyl)trinuoroacetamide, with 1% tert.butyldimethylchlorosilane as catalyst, to prepare the tert.-butyldimethylsilyl amino acid derivatives. Alkylsilylation

High resolution capillary gas chromatogr
High resolution capillary gas chromatography and gas chromatography-mass spectrometry of protein and non-protein amino acids, amino alcohols, and hydroxycarboxylic acids as theirtert-butyldimethylsilyl derivatives
✍ Šimek, Petr ;Heydová, Anna ;Jegorov, Alexandr 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 784 KB

## Abstract A simple, single‐step derivatization technique is presented for capillary GC‐FID and GC‐MS separation and identification of common protein and non‐protein constituents of natural peptides as their __tert__‐butyldimethylsilyl (TBDMS) derivatives. The __tert__‐butyldimethyl‐silylation of