In the title compound, C 16 H 36 N + ÁC 24 BF 20 À , the geometric parameters do not show any unusual values. The four n-butyl chains adopt an all-trans conformation.
Butylammonium tetrahydroxypentaborate
✍ Scribed by Pan, Chun-Yang ;Wang, Guo-Ming ;Zheng, Shou-Tian ;Yang, Guo-Yu
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 213 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
packing of the cations and anions in the crystal structure, there are no other signi®cant interactions (Fig. 2).
In the title compound, C 4 H 11 BrN + ÁBF 4 À , both ions lie on crystallographic mirror planes, and the compound is isomorphous with the chloromethyl analog. The C-Br distance is 1.927 (2) A ˚.
The structure of the title compound, C 16 H 36 N + ÁPF 6 À , has been reported previously by Angaridis, Cotton & Petrukhina [Inorg. Chim. Acta (2001), 324, 318±323]. However, these authors found the PF 6 À ion to be heavily disordered and they did not publish any coordinates. We present here a redet
Single-crystal X-ray study T = 100 K Mean (C-C) = 0.007 A Disorder in solvent or counterion R factor = 0.041 wR factor = 0.095 Data-to-parameter ratio = 29.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.