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Bridged Hemilabile Allylphosphonate Ligand: Synthesis and Crystal Structure of a New Binuclear Rhodium Complex

✍ Scribed by Le Gall, Irène; Laurent, Pascale; Toupet, Loïc; Salaün, Jean-Yves; des Abbayes, Hervé

Book ID
121221458
Publisher
American Chemical Society
Year
1997
Tongue
English
Weight
140 KB
Volume
16
Category
Article
ISSN
0276-7333

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✍ John Springborg; Margareta Zehnder 📂 Article 📅 1984 🏛 John Wiley and Sons 🌐 German ⚖ 449 KB

The reaction of the ammonia diol [(NH,)4Rh(OH)2Rh(NH,),]4' with H,O, yields among other products a peroxo-bridged dimeric species [(NH,),Rh(O,)(OH) Rh(NH,),(H,O)](ClO,),. Its structure was determined by single-crystal X-ray diffraction. The crystals are monoclinic with space group P2,/n and lattice