In the title compound, C 30 H 28 N 2 S 4 , the S-S bond length is 1.9910 (13) A ˚. In the absence of classical hydrogen bonds and interactions, the crystal packing is stabilized by van der Waals forces.
Bis(N-isopropyl-N-phenylthiocarbamoyl) disulfide
✍ Scribed by Raya, Indah ;Baba, Ibrahim ;Rosli, Fatimatul Z. ;Yamin, Bohari M.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 156 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The NCS 2 groups in the title compound, C 20 H 23 N 2 S 4 , are approximately perpendicular to each other, forming a dihedral angle of 80.10 (7) . The S-S bond length is 2.0086 (14) A ˚and the distance between the two terminal S atoms is 3.940 (3) A ˚.
📜 SIMILAR VOLUMES
In the crystal structure of the title compound, C~14~H~11~FN~2~OS, the molecules form centrosymmetric hydrogen-bonded dimers, with the S atom forming an intermolecular hydrogen bond with the H atom of an NH group.
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.047 wR factor = 0.114 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.