𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Bis(N-isopropyl-N-phenyl­thio­carbamo­yl) disulfide

✍ Scribed by Raya, Indah ;Baba, Ibrahim ;Rosli, Fatimatul Z. ;Yamin, Bohari M.


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
156 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


The NCS 2 groups in the title compound, C 20 H 23 N 2 S 4 , are approximately perpendicular to each other, forming a dihedral angle of 80.10 (7) . The S-S bond length is 2.0086 (14) A ˚and the distance between the two terminal S atoms is 3.940 (3) A ˚.


📜 SIMILAR VOLUMES


Bis(N,N-dibenzyl­thio­carbamo­yl) disulf
✍ Zhai, Jun ;Yin, Han-Dong ;Li, Feng ;Chen, Shao-Wen ;Wang, Da-Qi 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 122 KB

In the title compound, C 30 H 28 N 2 S 4 , the S-S bond length is 1.9910 (13) A ˚. In the absence of classical hydrogen bonds and interactions, the crystal packing is stabilized by van der Waals forces.

N-(N-Phenyl­benzimido­yl)thio­benzanilid
✍ Naumov, Pan˘ce ;Ristovska, Nata˘sa ;Anastasova, Frosa ;Ng, Seik Weng 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 182 KB
N-(3-Flurobenzo­yl)-N′-phenyl­thio­urea
✍ Zhang, You-Ming ;Qin, Jing-Dong ;Lin, Qi ;Wei, Tai-Bao 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 243 KB

In the crystal structure of the title compound, C~14~H~11~FN~2~OS, the molecules form centrosymmetric hydrogen-bonded dimers, with the S atom forming an intermolecular hydrogen bond with the H atom of an NH group.

Bis(μ-N-methyl-N-phenyl­di­thio­carbamat
✍ Baba, Ibrahim ;Lee, Lay Hoon ;Farina, Yang ;Othman, A. Hamid ;Ibrahim, Abdul Raz 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.047 wR factor = 0.114 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.