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Bis­(di-2-pyridyl­methanediol-κ3N,O,N′)copper(II) di­acetate tetrahydrate

✍ Scribed by Reinoso, Santiago ;Vitoria, Pablo ;San Felices, Leire ;Lezama, Luis ;Gutiérrez-Zorrilla, Juan M.

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
374 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.049 wR factor = 0.115 Data-to-parameter ratio = 21.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The Mn atom in the title compound, [Mn(C 11 H 10 N 2 O 2 ) 2 ]-(CH 3 CO 2 ) 2 Á4H 2 O, which lies on a centre of inversion, displays a tetragonally distorted octahedral coordination. The compound is isostructural with the analogous copper complex [Reinoso, Vitoria, San Felices, Lezama & Gutie ´rrez-

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê Disorder in main residue R factor = 0.039 wR factor = 0.095 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.