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Bis­[4-(tri­methyl­ammonio)­phenyl] di­sulfide tetra­iodo­mercurate(II)

✍ Scribed by Chen, Jin-Xiang ;Zhang, Wen-Hua ;Ren, Zhi-Gang ;Zhang, Yong ;Lang, Jian-Ping

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
252 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 193 K Mean '(C±C) = 0.009 A Ê R factor = 0.041 wR factor = 0.101 Data-to-parameter ratio = 25.7

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title complex, (C 6 H 18 N 2 )[V 2 Cl 5 (C 6 H 16 N 2 ) 2 ](C 24 H 20 B).-C 4 H 8 O, was prepared by the reaction of [V 2 Cl 3 (THF) 6 ](BPh 4 ) with [FeCl 2 (tmeda) 2 ] in the presence of one equivalent of tmeda (tmeda = N,N,N H ,N H -tetramethylethylenediamine) in methanol. The crystal structu