The silole ring of the title compound, C~22~H~46~OSi~3~, is planar. Geometric parameters do not show unusual values. The H atom and the hydroxy group on the silole Si atom are mutually disordered.
Bis(2-hydroxy-1-naphthaldehyde) oxaloyldihydrazone dihydrate
✍ Scribed by Zhu, Li-Na ;Li, Chang-Qing ;Li, Xiao-Zeng ;Li, Rong
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 196 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean (C-C) = 0.004 A R factor = 0.053 wR factor = 0.135 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The first independent molecule of (I), showing 35% probability displacement ellipsoids.
The molecule of the title compound, C 12 H 10 O 2 , is planar, with an intramolecular O-HÁ Á ÁO hydrogen bond between the hydroxy group and the carbonyl O atom. The structure is stabilized by intermolecular C-HÁ Á Á and offsetstacking interactions.
In the title compound, C 20 H 32 N 5 O 8 PÁ2H 2 O, molecules are linked to each other via intermolecular N-HÁ Á ÁO, N-HÁ Á ÁN, O-HÁ Á ÁO and O-HÁ Á ÁN hydrogen bonds with the water molecules acting as both acceptors and donors.