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Asymmetric Synthesis of the C14-C26 Building Block of Eribulin Mesylate

โœ Scribed by Murthy, Akondi Srirama; Mahipal, Bodugum; Chandrasekhar, Srivari

Book ID
118235087
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
572 KB
Volume
2012
Category
Article
ISSN
1434-193X

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Synthesis of kryptogenin-26-14C and dios
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โœ Raymond D. Bennett; Horst H. Sauer; Erich Heftmann ๐Ÿ“‚ Article ๐Ÿ“… 1969 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 444 KB

Kryptogenin-26-I4C (13) was synthesized from dihydrodiosgenin diacetate (1). The radioactive carbon atom was introduced by the Arndt-Eistert method, and the extra carbon atom was then removed by a carboxy-inversion reaction. Diosgenin-26-I4C (14) was prepared by reduction of kryptogenir~-26-~~C.