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Assignments of the 1H and 13C NMR spectra of trans-4-hydroxy-N-9-fluorenylmethoxycarbonyl-L-proline using one- and two-dimensional NMR spectroscopy

✍ Scribed by Dagfinn W. Aksnes; George W. Francis; Dionissios Papaioannou

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
161 KB
Volume
31
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The ^1^H and ^13^C NMR spectra of trans‐4‐hydroxy‐N‐9‐fluorenylmethoxycarbonyl‐L‐proline show a 56:44 mixture of two conformers due to hindered rotation around the partial CN double bond. A combination of homo‐ and heteronuclear 1 D and 2D NMR techniques provided the assignments of the ^1^H and ^13^C resonances.

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