The total assignment of the 13C and the ' H NMR spectra of four derivatives of 1,3diaza-2,4-diboranaphthalene has been performed. The interpretation of the spectra was achieved from the concerted application of direct and long-range heteronuclear chemical shift correlation and homonuclear COSY two-d
Assignment of the 1H and 13C NMR spectra of naphtho [1′,2′:4,5]thieno[2,3-c]quinoline using two-dimensional NMR spectroscopy
✍ Scribed by Lyle W. Castle; Andrew S. Zektzer; Milton D. Johnston Jr.
- Publisher
- John Wiley and Sons
- Year
- 1992
- Tongue
- English
- Weight
- 470 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
The ^1^H NMR spectrum of naphtho [1′,2′:4,5]thieno[2,3‐c]quinoline is highly congested because all the protons are in an aromatic environment, and the structure of the molecule is nearly symmetric. With this in mind, the assignment of the ^1^H and ^13^C NMR spectra of this compound obtained using two‐dimensional NMR spectroscopy is reported.
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