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Structural assignment of the 1H and 13C NMR spectra of 3-Cyano-1,2,2-trimethyl-6-azatricyclo [3.3.1.03,8] non-6-ene using two-dimensional NMR spectroscopy

✍ Scribed by Tullio Caronna; Daniela Dal Pio Luogo

Publisher: John Wiley and Sons
Year: 1994
Tongue: English
Weight: 171 KB
Volume: 32
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1260320314

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✦ Synopsis

Abstract

^1^H NMR of the tricyclic molecule 3 ‐ Cyano ‐1,2,2‐ trimethyl ‐ 6 ‐ azatricyclo ‐[3.3.1.0^3,8^]non‐6‐ene does not permit the distinction between this structure and the other regioisomer that can be formed in a photochemically induced reaction. The elucidation of the structure was possible via the assignment of the ^1^H and ^13^C NMR spectra of this compound obtained using two‐dimensional NMR spectroscopy.

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