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1H and 13C spectral assignment of naphtho[2′,1′:5,6]-naphtho[2′,1′:4,5]thieno[2,3-c]quinoline using the IDR-GHSQC-TOCSY experiment

✍ Scribed by Chad E. Hadden; Gary E. Martin; J.-K. Luo; Raymond N. Castle


Publisher
Journal of Heterocyclic Chemistry
Year
2000
Tongue
English
Weight
306 KB
Volume
37
Category
Article
ISSN
0022-152X

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✦ Synopsis


Abstract

The assignment of the NMR spectra of the polynuclear heteroaromatic naphtho[2′,1′:5,6]naphtho‐[2′,1′:4,5]thieno[2,3‐c]quinoline is reported. The analysis was based on the homonuclear ROESY, heteronuclear direct GHSQC, IDR‐GHSQC‐TOCSY, and long‐range GHMBC experiments. The complete ^1^H and ^13^C shift assignments are reported.


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