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14N NMR and Two-Dimensional Suspension 1H and 13C HRMAS NMR Spectroscopy of Ionic Liquids Immobilized on Silica

✍ Scribed by Stefano Brenna; Tobias Posset; Julien Furrer; Janet Blümel

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
270 KB
Volume
12
Category
Article
ISSN
0947-6539

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✦ Synopsis

Abstract

A variety of popular ionic liquids have been synthesized and characterized, including by optimized ^14^N NMR spectroscopy of the neat and dissolved ionic liquids. Ionic liquids incorporating Si(OEt)~3~ groups have been immobilized on silica in a well‐defined manner with the imidazolium moiety remaining intact. This has been proved by optimized one‐ and two‐dimensional ^1^H and ^13^C HRMAS NMR spectroscopy of the materials suspended in suitable solvents.

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