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Applications of two-dimensional NMR in spectral assignments of some friedelanes and secofriendelanes

✍ Scribed by Amarendra Patra; Swapan K. Chaudhuri; Aditi K. Acharyya

Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
325 KB
Volume
28
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Carbon‐13 spectral assignments of three friedelanes and nineteen secofriedelanes have been made from mutual correlations, 2D X‐H correlation analyses and comparison with the carbon shifts of friedelin, which were firmly established by an INADEQUATE experiment that required reassignment of some of its resonances. Specific methyl and methine proton resonance assignments for some friedelanes, established from X‐H correlation studies, are also reported.

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