Analysis of lipoic acid in biological samples by gas chromatography with flame photometric detection
โ Scribed by Hiroyuki Kataoka; Noritoshi Hirabayashi; Masami Makita
- Publisher
- Elsevier Science
- Year
- 1993
- Weight
- 536 KB
- Volume
- 615
- Category
- Article
- ISSN
- 0378-4347
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Pulsed flame photometric detection (PFPD) for gas chromatography was applied to organotin compounds as standards and in environmental samples. Ethylated organotin species (n-propyl-, n-butyl-and phenyl-) were extracted from spiked artificial seawater and from an environmental sample. Selectivity tow
A method has been developed for the gas chromatographic analysis of lipoic acid in biological samples. The lipoic acid is released from the samples by acid hydrolysis in the presence of the internal standatds 1,2-dithiolane-3-butyric acid and/or 1,2-dithiolane-3caproic acid. After hydrolysis, the li