Linalool, nerol, geraniol, citronellol and a-terpineol were phosphorylated and the products purified by adsorption chromatography on XAD-2. High performance liquid chromatography-tandem mass spectrometry (LC-MSMS) analysis using the electrospray ionization technique (ESI) revealed the occurrence of
Analysis of furanocoumarins from Yemenite Dorstenia species by liquid chromatography/electrospray tandem mass spectrometry
✍ Scribed by Ramona Heinke; Katrin Franke; Katharina Michels; Ludger Wessjohann; Nasser Abdullah Awadh Ali; Jürgen Schmidt
- Publisher
- John Wiley and Sons
- Year
- 2012
- Tongue
- English
- Weight
- 590 KB
- Volume
- 47
- Category
- Article
- ISSN
- 1076-5174
- DOI
- 10.1002/jms.2017
No coin nor oath required. For personal study only.
✦ Synopsis
A series of prevailing prenylated furanocoumarins from leaves of Dorstenia gigas and Dorstenia foetida (Moraceae) were investigated by liquid chromatography/electrospray tandem mass spectrometry. The mass spectral behavior of the furanocoumarins under positive ion electrospray conditions is discussed using both an ion trap and a triple quadrupole system. It is demonstrated that both methods represent valuable tools not only for the rapid classification of this type of compounds, but also with respect to their substitution pattern. Copyright © 2012 John Wiley & Sons, Ltd.
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