Analysis of conjugated bile acids by high performance liquid chromatography and mass spectrometry
β Scribed by G. Mingrone; A. V. Greco; L. Boniforti; S. Passi
- Book ID
- 112772951
- Publisher
- Springer-Verlag
- Year
- 1983
- Tongue
- English
- Weight
- 328 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0024-4201
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π SIMILAR VOLUMES
Major conjugated bile acids of human bile have been resolved by high-pressure liquid chromatography. The elutions are carried out in two stages on Corasil II or PPorasil columns; first, an alkaline solvent system (Zpropanokethyl acetate/ water/7 N ammonium hydroxide, 260:600:50:3) was used for separ
A rapid method was developed for the analysis of polar conjugated bile acids by combined packed column supercritical fluid chromatography/mass spectrometry. Direct coupling of the column to the mass spectrometer was effected with a modified thermospray interface operated in the filament-on mode. Max