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An Improved Synthesis of Citric Acid-1,5-C 14 1

✍ Scribed by Rothchild, Seymour; Fields, Melvin


Book ID
126833009
Publisher
American Chemical Society
Year
1952
Tongue
English
Weight
130 KB
Volume
74
Category
Article
ISSN
0002-7863

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## Abstract Uracil‐6‐^14^C (**7**). prepared in high radiochemical yield by conventional methods. has been converted to 5‐fluororacil ‐6‐^14^C (**9**) in over 90% yield using trifluoromethylhypofluorite. The use of this recently introduced reagent eliminates the necessity of preparing **9** from fl