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An Expedient Synthesis of Olfactory Lactones by Intramolecular Hydroacylalkoxylation Reactions

✍ Scribed by Luis A. Adrio; King Kuok (Mimi) Hii

Book ID
102174162
Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
296 KB
Volume
2011
Category
Article
ISSN
1434-193X

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The Ugi four-component condensation between 5-oxo-3-thiacarboxylic acids, benzylamines and cyclohexyl isocyanide gave 5-oxothiomorpholine-3-carboxamides. The configuration of bicyclic thiomorpholine derivatives was established by NOESY experiments.