✦ LIBER ✦

Synthesis of thiomorpholines by an intramolecular Ugi reaction

✍ Scribed by Stefano Marcaccini; Roberto Pepino; Tomás Torroba; Daniel Miguel; Marı́a Garcı́a-Valverde

Book ID: 104252260
Publisher: Elsevier Science
Year: 2002
Tongue: French
Weight: 97 KB
Volume: 43
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(02)02064-6

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✦ Synopsis

The Ugi four-component condensation between 5-oxo-3-thiacarboxylic acids, benzylamines and cyclohexyl isocyanide gave 5-oxothiomorpholine-3-carboxamides. The configuration of bicyclic thiomorpholine derivatives was established by NOESY experiments.

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