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An Efficient Synthesis of (Fluoromethyl)pyridylamines for Labeling with Fluorine-18

✍ Scribed by Lee, Kyo Chul; Chi, Dae Yoon


Book ID
111654727
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
79 KB
Volume
64
Category
Article
ISSN
0022-3263

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An efficient procedure for the synthesis
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## Abstract A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^O‐labelled hexamethyldisiloxane in this reaction results in the formation of ^18^O‐