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An efficient procedure for the synthesis of 18O-labelled methanesulfinyl chloride

✍ Scribed by Józef Drabowicz; Bogdan Bujnicki; Marian Mikolajczyk

Publisher
John Wiley and Sons
Year
2003
Tongue
French
Weight
80 KB
Volume
46
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^O‐labelled hexamethyldisiloxane in this reaction results in the formation of ^18^O‐labelled methanesulfinyl chloride. Copyright © 2003 John Wiley & Sons, Ltd.

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