## Abstract A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^O‐labelled hexamethyldisiloxane in this reaction results in the formation of ^18^O‐
✦ LIBER ✦
An improved procedure for the synthesis of [18O]sulfoxides
✍ Scribed by Andrzej Okruszek
- Publisher
- John Wiley and Sons
- Year
- 1983
- Tongue
- French
- Weight
- 139 KB
- Volume
- 20
- Category
- Article
- ISSN
- 0022-2135
No coin nor oath required. For personal study only.
✦ Synopsis
180]SuIfozides are prepared i n high y i e l d with no loss of isotope enrichment by one-step s u l f i d e oxidation with CHgC12/Br2/H2180/pyridine.
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