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An Efficient Procedure for Microscale Synthesis of Semicarbazones

✍ Scribed by Pandita, Sangeeta; Goyal, Samta; Arif, Nadira; Passey, Sarita


Book ID
120081528
Publisher
American Chemical Society
Year
2004
Tongue
English
Weight
57 KB
Volume
81
Category
Article
ISSN
0021-9584

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An efficient procedure for the synthesis
✍ JΓ³zef Drabowicz; Bogdan Bujnicki; Marian Mikolajczyk πŸ“‚ Article πŸ“… 2003 πŸ› John Wiley and Sons 🌐 French βš– 80 KB πŸ‘ 1 views

## Abstract A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^O‐labelled hexamethyldisiloxane in this reaction results in the formation of ^18^O‐