An Efficient Microscale Procedure for the Synthesis of Aspirin
β Scribed by Pandita, Sangeeta; Goyal, Samta
- Book ID
- 120325257
- Publisher
- American Chemical Society
- Year
- 1998
- Tongue
- English
- Weight
- 48 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0021-9584
No coin nor oath required. For personal study only.
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## Abstract A new procedure for the synthesis of methanesulfinyl chloride is described which involves chlorination of dimethyl disulfide with sulfuryl chloride in the presence of hexamethyldisiloxane. The use of ^18^Oβlabelled hexamethyldisiloxane in this reaction results in the formation of ^18^Oβ
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