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An Efficient Enantioselective Synthesis of Blastmycinone.

✍ Scribed by Yong-Qing Yang; Yi-Kang Wu

Publisher
John Wiley and Sons
Year
2006
Weight
18 KB
Volume
37
Category
Article
ISSN
0931-7597

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An Efficient Enantioselective Synthesis
An Efficient Enantioselective Synthesis of Blastmycinone
✍ Yong-Qing Yang; Yi-Kang Wu πŸ“‚ Article πŸ“… 2005 πŸ› John Wiley and Sons 🌐 English βš– 98 KB

## Abstract Blastmycinone, a degradation product of the antibiotic antimycin A, was synthesized with a TiCl~4~‐mediated asymmetric aldolization as the key step. Some unexpected yet interesting chemistry was also observed.

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The numbering of 1 corresponds to [2] and is used also for all intermediates; systematic names are given in the Exper. Part. ## ') For the cleavage of cdrboxylates with lithiated alkylsulfones, see [9].