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An Anomalous Endohedral Structure of Eu@C82 Metallofullerenes

โœ Scribed by Bao-Yun Sun; Toshiki Sugai; Eiji Nishibori; Kenichi Iwata; Makoto Sakata; Masaki Takata; Hisanori Shinohara

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
428 KB
Volume
44
Category
Article
ISSN
0044-8249

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Preparation and characterization of the
Preparation and characterization of the endohedral metallofullerene Lu@C82
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A new metallofullerene Lu@C 82 has been isolated with good purity using polar solvent extraction and HPLC techniques. XPS, EPR and UV-Vis-Nir spectroscopic techniques are employed to characterize the mono-metallofullerene Lu@C 82 . Our results suggest that the encaged Lu atom donates approximately t

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La@C 82 is recognized by an isophthaloyl-bridged porphyrin dimer forming a stable 1:1 supramolecular complex with an association constant K assoc = (67.3 ยฑ 3.2) ร‚ 10 3 M ร€1 .