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Alkylphosphonic dichlorides, new reagents for the enantiomeric excess determination of chiral alcohols and thiols by 31P NMR

✍ Scribed by Ben L. Feringa; Ab A. Smaardijk; Hans Wynberg; Bert Strijtveen; Richard M. Kellogg

Publisher
Elsevier Science
Year
1986
Tongue
French
Weight
210 KB
Volume
27
Category
Article
ISSN
0040-4039

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An efficient chiral phosphorus derivatiz
An efficient chiral phosphorus derivatizing agent for the determination of the enantiomeric excess of chiral alcohols and amines by 31P NMR spectroscopy
✍ Kang Ying Li; Zheng Hong Zhou; Albert. S. C. Chan; Chu Chi Tang πŸ“‚ Article πŸ“… 2002 πŸ› John Wiley and Sons 🌐 English βš– 120 KB πŸ‘ 1 views

## Abstract The chiral phosphorus derivatizing agent (CDA) 1 was prepared from optically pure (S)‐__1,1‐bis‐2‐naphthol__. It was first used in the determination of the enantiomeric excess of chiral alcohols and amines by means of ^31^P NMR spectroscopy. It showed that, for the chiral aromatic alcoh