Acyl Derivatives of Aldoses. II. Derivatives of D-glycero-D-galacto-Heptose and D-Galactose
β Scribed by Lederkremer, Rosa Muchnik de; Deferrari, Jorge O.
- Book ID
- 126172271
- Publisher
- American Chemical Society
- Year
- 1962
- Tongue
- English
- Weight
- 391 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0022-3263
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The analysis of a range of methyl ethers derived from methyl 7-deoxy-Dglycero-go-galacfo-heptopyranoside (1) and methyl 7-deoxy-L-gfycero-pDgulucto-heptopyranoside (2) is examined in relation to their retention times in opentubular gas-liquid chromatography, and to their electron-impact mass spect
Treatment of a solution of 3-deoxy-o-glycero-D-galacto-non-2-ulosonic (ICDN) in 11 N aqueous hydrochloric acid with an excess of ethanethiol gave in 52% yield the diethyl dithioacetal of the corresponding l,Clactone, which was further characterized as its peracetate. With 1,3\_propanedithiol, only o