𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Accurate Determination of Order Parameters from 1 H, 15 N Dipolar Couplings in MAS Solid-State NMR Experiments

✍ Scribed by Chevelkov, Veniamin; Fink, Uwe; Reif, Bernd


Book ID
126881024
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
936 KB
Volume
131
Category
Article
ISSN
0002-7863

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Determination of the Peptide Torsion Ang
✍ M. Hong; J.D. Gross; W. Hu; R.G. Griffin πŸ“‚ Article πŸ“… 1998 πŸ› Elsevier Science 🌐 English βš– 214 KB

We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15

Order parameters based on 13C1H, 13C1H2
✍ Justin Lorieau; Ann E. McDermott πŸ“‚ Article πŸ“… 2006 πŸ› John Wiley and Sons 🌐 English βš– 506 KB

Order parameters describing conformational exchange processes on the nanosecond to microsecond timescale can be obtained from powder patterns in solid-state NMR (SSNMR) experiments. Extensions of these experiments to magic-angle spinning (MAS) based high-resolution experiments have been demonstrated