A novel series of hydrogen-bonded solid 1 : 1 acid-base complexes of 15 N-labeled 2,4,6-trimethylpyridine (collidine) with carboxylic acids and their hydrogen bond deuterated analogs were synthesized and studied by 1 H magic angle spinning (MAS) and 15 N cross-polarization NMR with and without MAS.
✦ LIBER ✦
2H Chemical-shift resolution and dipolar2H-1H,2H-15N correlations in solid-state MAS NMR spectroscopy for structure determination and distance measurements in hydrogen-bonded systems
✍ Scribed by Martin Schulz-Dobrick; Ingo Schnell
- Book ID
- 110553755
- Publisher
- SP Versita
- Year
- 2005
- Tongue
- English
- Weight
- 312 KB
- Volume
- 3
- Category
- Article
- ISSN
- 1895-1066
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