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A two-step synthesis of benzylamine-15N from ammonia-15N

โœ Scribed by C. Gazzola; G. L. Kenyon

Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
149 KB
Volume
15
Category
Article
ISSN
0022-2135

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โœฆ Synopsis

The reaction o f amnonia-l5N w i t h benzaldehyde i n 50% aq. methanol followed by slow removal o f solve t l e d t o a high y i e l d o f a c r y s t a l l i n e product (benzylimine-r5N).

On reduction with sodium cyanoborohydride a good y i e l d o f benzylamine-15N was obtained. The syntheti c usefulness o f t h i s compound i s discussed.

๐Ÿ“œ SIMILAR VOLUMES

A convenient synthesis of creatine-15N f
A convenient synthesis of creatine-15N from glycine-15N via sarcosine-15N
โœ W. Greenaway; F. R. Whatley ๐Ÿ“‚ Article ๐Ÿ“… 1978 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 184 KB

The pre aration of creatine-' 5N monohydrate from intermediate is described. 15N) is converted to benzenesulphonyl glycine-I 5N, which is methylated to give benzenesulphonyl sarcosine--l5N. The latter is hydrolysed to sarcosine-l 5N1 which is isolated by ion exchange chromatography. Sarcosine-l5N i