๐”– Bobbio Scriptorium
โœฆ   LIBER   โœฆ

A Two-Step, One-Pot Enzymatic Synthesis of 2-Substituted 1,3-Diols

โœ Scribed by Kalaitzakis, Dimitris; Smonou, Ioulia

Book ID
119945830
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
814 KB
Volume
75
Category
Article
ISSN
0022-3263

No coin nor oath required. For personal study only.

๐Ÿ“œ SIMILAR VOLUMES

One-Pot Two-Steps Synthesis of 1,2-Diol
One-Pot Two-Steps Synthesis of 1,2-Diol
โœ Fringuelli, F.; Germani, R.; Pizzo, F.; Savelli, G. ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Taylor and Francis Group ๐ŸŒ English โš– 155 KB
A one-pot, two step synthesis of 2,2-dis
A one-pot, two step synthesis of 2,2-disubstituted 1-nitroalkenes
โœ Yeong-Jiunn Jang; Wen-Wei Lin; Yuh-Kuo Shih; Ju-Tsung Liu; Ming-Hsing Hwang; Chi ๐Ÿ“‚ Article ๐Ÿ“… 2003 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 303 KB

The reactions of ketones 1a -o, nitromethane 2, and a stoichiometric amount of piperidine 3a or ethylenediamine 3b in the presence of mercaptan 6a in THF or CH 3 CN solution give high yields of b-nitrosulfides 7a -o. The latter can be oxidized by 8a (m-CPBA or m-CPBA/AcOH) at 08C, 8b (H 2 O 2 /AcOH)