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A Three-Step Preparation of Dihydroxyacetone Phosphate Dimethyl Acetal †

✍ Scribed by Ferroni, Edward L.; DiTella, Victoria; Ghanayem, Nancy; Jeske, Rebecca; Jodlowski, Christopher; O'Connell, Matthew; Styrsky, Jennifer; Svoboda, Robyn; Venkataraman, Ajay; Winkler, Beth M.

Book ID
125517493
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
59 KB
Volume
64
Category
Article
ISSN
0022-3263

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A three-step preparation of MAC reagents
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✍ Hisao Nemoto; Xinming Li; Rujian Ma; Ichiro Suzuki; Masayuki Shibuya 📂 Article 📅 2003 🏛 Elsevier Science 🌐 French ⚖ 126 KB

An alternative method for the preparation of MAC reagents, H-C(CN) 2 O-R, was developed. Using the proposed method, MAC reagents with acyl moiety were synthesized from malononitrile in more than 60% overall yields in three steps.