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A synthesis of some pyridinylpyrimidines from ketenedithioacetals

✍ Scribed by Ruth B. Katz; Michael B. Mitchell; Peter G. Sammes; Robert J. Ife


Book ID
108371507
Publisher
Elsevier Science
Year
1989
Tongue
French
Weight
691 KB
Volume
45
Category
Article
ISSN
0040-4020

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Stereoselective synthesis of hydroxy-ket
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The reaction of Garner's aldehyde with dithioacetate enethiolates followed by alkylation of the intermediate aldolate gives hydroxy-ketenedithioacetals with a moderate anti selectivity. This methodology was applied to the synthesis of various other ketene dithioacetals with high E or Z stereoselecti