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Fluorinated ketenedithioacetals. 5. A new synthesis of perfluoroketenedithioacetals from alkyl perfluoroalkanedithiocarboxylates

✍ Scribed by Charles Portella; Yuri Shermolovich

Book ID
104257160
Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
165 KB
Volume
38
Category
Article
ISSN
0040-4039

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πŸ“œ SIMILAR VOLUMES

Fluorination at C5β€² of nucleosides. Synt
Fluorination at C5β€² of nucleosides. Synthesis of the new class of 5β€²-fluoro-5β€²-S-aryl (alkyl) thionucleosides from adenosine.
✍ Morris J. Robins; Wnuk F. Stanislaw πŸ“‚ Article πŸ“… 1988 πŸ› Elsevier Science 🌐 French βš– 248 KB

Treatment of protected 5'-S-aryl (alkyl) thioadenosine sulfoxides (3) with diethylaminosulfur trifluoride (DAST)/antimony trichloride (SbC13) and deprotection resulted in high-yield syntheses of the new 5'-fluoro-5'-S-aryl (alkyl) thioadenosines (5).