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A Simple Method to Prepare Alkyl 3,5-Dioxohexanoates

✍ Scribed by Yuste, Francisco; Breña, Francisco Kuri; Barrios, Héctor; Sánchez-Obregón, Rubén; Ortíz, Benjamín; Walls, Fernando

Book ID
120214634
Publisher
Taylor and Francis Group
Year
1988
Tongue
English
Weight
169 KB
Volume
18
Category
Article
ISSN
0039-7911

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✍ Chunhua Yang; Mark S Jensen; David A Conlon; Nobuyoshi Yasuda; David L Hughes 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 73 KB

A simple and scalable method for the preparation of a potentially versatile organostannane, 1-aza-5chloro-5-stannabicyclo[3.3.3]undecane (1), is described. Stannane 1 was prepared by the disproportionation of N(CH 2 CH 2 CH 2 SnBu 3 ) 3 and SnCl 4 at 70-100°C. This reaction requires the addition of