𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A second polymorph of (5,10,15,20-tetra­phenyl­porphyrinato)copper(II)

✍ Scribed by He, Hong-Shan

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
191 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the title compound, [Cu(C 44 H 28 N 4 )], the copper ion is located at the center of the centrosymmetric and perfectly planar porphyrin ring.

📜 SIMILAR VOLUMES

[5,10,15,20-Tetrakis(2,6-dimethoxyphenyl
[5,10,15,20-Tetrakis(2,6-dimethoxyphenyl)porphyrinato]nickel(II)–toluene–dichloromethane (3/2/4):a mixed solvate
✍ Conrad, Diane ;DeCoskey, Jennifer ;Yeisley, Christopher ;Zeller, Matthias ;Hunte 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 778 KB

The crystal structure, electronic spectroscopy, and ^1^H NMR data for the title compound, [Ni(C~52~H~44~N~4~O~8~)]·0.67C~7~H~8~·1.33CH~2~Cl~2~, are reported. The compound was prepared by the reaction of nickel(II) acetate with the ligand in refluxing glacial acetic acid. The asymmetric unit consists

Synchrotron X-ray study of [5,15-di­phen
Synchrotron X-ray study of [5,15-di­phenyl-2,8,12,18-tetra-n-hexyl-3,7,13,17-tetra­methyl­porphyrinato]­nickel(II)
✍ Bond, Andrew D. ;Feeder, Neil ;Redman, James E. ;Teat, Simon J. ;Sanders, Jeremy 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 533 KB

Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.003 A Ê R factor = 0.052 wR factor = 0.129 Data-to-parameter ratio = 23.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.