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A rapid, mild and acid-free procedure for the preparation of acyl chlorides including formyl chloride

✍ Scribed by G.B. Villeneuve; T.H. Chan

Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
257 KB
Volume
38
Category
Article
ISSN
0040-4039

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The reaction of lithium ester enolates w
The reaction of lithium ester enolates with acid chlorides. A convenient procedure for the preparation of Ξ²-keto esters
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Lithium ester enolates, prepared by the reaction of lithium N-isopropylcyclohexylamide (LIICA) with esters at -78' (eq. 1); react with acid chlorides at this same low temperature to provide satisfactory yields of the corresponding S-keto esters (eq. II). This procedure represents an exceedingly vers