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A preparative isolation and purification of arctigenin and matairesinol from Forsythia koreana by centrifugal partition chromatography

✍ Scribed by Chul Young Kim; Mi-Jeong Ahn; Jinwoong Kim

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
595 KB
Volume
29
Category
Article
ISSN
1615-9306

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✦ Synopsis

A preparative isolation and purification of arctigenin and matairesinol from Forsythia koreana by centrifugal partition chromatography Centrifugal partition chromatography was applied to separate arctigenin and matairesinol from Forsythia koreana extract with a two-phase solvent system composed of n-hexane-ethyl acetate-methanol-water (5 : 5 : 5 : 5 v/v). Using this method, arctigenin and matairesinol were successfully separated from partially purified F. koreana extracts in only one step. The purities of isolated compounds were determined to be over 90% by HPLC analysis.

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